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Investigation of thermal behavior of mixed-valent iron borates vonsenite and hulsite containing [OM<inf>4</inf>]<sup>n+</sup>and [OM <inf>5</inf>] <sup>n+</sup>oxocentred polyhedra by in situ high-temperature Mössbauer spectroscopy, X-ray diffraction and thermal analysis 217

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Investigation of thermal behavior of mixed-valent iron borates vonsenite and hulsite containing [OM<inf>4</inf>]<sup>n+</sup>and [OM <inf>5</inf>] <sup>n+</sup>oxocentred polyhedra by in situ high-temperature Mössbauer spectroscopy, X-ray diffraction and thermal analysis 1 1 5 14 12 19 1

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