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Tracking of the formation of binuclear nickel complexes of [Ni<inf>2</inf>(µ-O<inf>2</inf>PR<sup>1</sup>R<sup>2</sup>)<inf>2</inf>(bpy)<inf>4</inf>]Br<inf>2</inf> type by ESI and MALDI mass spectrometry 242

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Tracking of the formation of binuclear nickel complexes of [Ni<inf>2</inf>(µ-O<inf>2</inf>PR<sup>1</sup>R<sup>2</sup>)<inf>2</inf>(bpy)<inf>4</inf>]Br<inf>2</inf> type by ESI and MALDI mass spectrometry 10 18 3 6 1 4 11

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