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The self-assembly of DyF<inf>3</inf> nanoparticles synthesized by chloride-based route

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dc.contributor.author Alakshin E.
dc.contributor.author Kondratyeva E.
dc.contributor.author Nuzhina D.
dc.contributor.author Iakovleva M.
dc.contributor.author Kuzmin V.
dc.contributor.author Safiullin K.
dc.contributor.author Gubaidullin A.
dc.contributor.author Kikitsu T.
dc.contributor.author Kono K.
dc.contributor.author Klochkov A.
dc.contributor.author Tagirov M.
dc.date.accessioned 2019-01-22T20:45:39Z
dc.date.available 2019-01-22T20:45:39Z
dc.date.issued 2018
dc.identifier.issn 1388-0764
dc.identifier.uri https://dspace.kpfu.ru/xmlui/handle/net/148634
dc.description.abstract © 2018, Springer Nature B.V. The series of DyF3 nanoparticles was synthesized for the first time by a chloride-based route, using the water-soluble dysprosium chloride hexahydrate as a precursor. The synthesized nanoparticles have sizes of 3 to 7 nm, which is the smallest reported size for DyF3 nanoparticles. The influence of precursor concentration in an aqueous solution prior to the chemical reaction on the size of nanoparticles was studied. The influence of microwave-assisted hydrothermal treatment was also studied. The analysis of transmission electron microscopy (TEM) data revealed no correlation between the size of synthesized nanoparticles and the concentration of the aqueous solution. The AC/DC magnetic susceptibility of DyF3 nanoparticles was measured. The dipolar ferromagnetic transition for this sample was not observed down to 1.8 K that can be possibly explained by onset of superparamagnetism. The self-assembly of DyF3 nanoparticles was observed for the first time by analysis of XRD and TEM data and the evidence of superlattice formation along (020) and (210) lattice planes over the size of 20–30 nm (4–5 nanoparticles) was obtained. [Figure not available: see fulltext.].
dc.relation.ispartofseries Journal of Nanoparticle Research
dc.subject Colloidal processing
dc.subject Crystal structure
dc.subject Electron microscopy
dc.subject Nanocrystalline materials
dc.subject Self-assembly
dc.subject X-ray techniques
dc.title The self-assembly of DyF<inf>3</inf> nanoparticles synthesized by chloride-based route
dc.type Article
dc.relation.ispartofseries-issue 12
dc.relation.ispartofseries-volume 20
dc.collection Публикации сотрудников КФУ
dc.source.id SCOPUS13880764-2018-20-12-SID85058786428


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  • Публикации сотрудников КФУ Scopus [20180]
    Коллекция содержит публикации сотрудников Казанского федерального (до 2010 года Казанского государственного) университета, проиндексированные в БД Scopus, начиная с 1970г.

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