One- and two-dimensional NMR study of structure of 1,2-disubstituted p-tert-butylthiacalix[4]arene containing amide fragment

dc.contributor.author	Karataeva F.
dc.contributor.author	Vagizova R.
dc.contributor.author	Stoikov I.
dc.contributor.author	Antipin I.
dc.contributor.author	Klochkov V.
dc.date.accessioned	2018-09-18T20:18:45Z
dc.date.available	2018-09-18T20:18:45Z
dc.date.issued	2013
dc.identifier.issn	1070-3632
dc.identifier.uri	https://dspace.kpfu.ru/xmlui/handle/net/138593
dc.description.abstract	The structure of 5,11,17,23-tetra-tert-butyl-25,27-dihydroxy-26,28-bis[N- (4′-nitrophenyl)aminocarbonylmethoxy] thiacalix[4]arene I was examined by 1D and 2D (NOESY) 1H and 13C NMR methods in a CDCl 3 solution using numerical simulation (semi-empirical quantum-chemical calculations, PM3 method). Compound I was found to exist in the 1,2-alternate conformation, where bulky substituents OCH2C(O) · NHPhNO2 are in the endo-position relative to the macrocycle cavity. © 2013 Pleiades Publishing, Ltd.
dc.relation.ispartofseries	Russian Journal of General Chemistry
dc.title	One- and two-dimensional NMR study of structure of 1,2-disubstituted p-tert-butylthiacalix[4]arene containing amide fragment
dc.type	Article
dc.relation.ispartofseries-issue	4
dc.relation.ispartofseries-volume	83
dc.collection	Публикации сотрудников КФУ
dc.relation.startpage	698
dc.source.id	SCOPUS10703632-2013-83-4-SID84878677407

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