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dc.contributor.author | Latypov S. | |
dc.contributor.author | Epifanova N. | |
dc.contributor.author | Popova E. | |
dc.contributor.author | Vasilevsky S. | |
dc.contributor.author | Solovieva S. | |
dc.contributor.author | Antipin I. | |
dc.contributor.author | Konovalov A. | |
dc.date.accessioned | 2018-09-18T20:10:48Z | |
dc.date.available | 2018-09-18T20:10:48Z | |
dc.date.issued | 2011 | |
dc.identifier.issn | 0937-9347 | |
dc.identifier.uri | https://dspace.kpfu.ru/xmlui/handle/net/137317 | |
dc.description.abstract | The combined application of two-dimensional nuclear magnetic resonance (2-D NMR) correlation experiments and gauge-including atomic orbital (GIAO) 13C NMR chemical shift calculations allowed reliable and simple determination of regioisomeric structure of heterocyclic substituents on the calix[4]arene lower rim. Moreover, the 1-D double pulsed field gradient nuclear Overhauser effect technique allows quick and efficient measurement of small nuclear Overhauser effects and, in doing so, establishes a 3-D structure of calix[4]arene simply and unequivocally. In general, these methods may find application in the regio- and stereoisomeric structure determination of complicated macrocyclic compounds. © 2011 Springer-Verlag. | |
dc.relation.ispartofseries | Applied Magnetic Resonance | |
dc.title | Combined Use of 2-D NMR Correlation Experiments, GIAO DFT 13C Chemical Shifts and 1-D NOESY Methods in Regioisomeric and Conformational Structure Determination of Cyclophanes in Solution | |
dc.type | Article | |
dc.relation.ispartofseries-issue | 2-4 | |
dc.relation.ispartofseries-volume | 41 | |
dc.collection | Публикации сотрудников КФУ | |
dc.relation.startpage | 467 | |
dc.source.id | SCOPUS09379347-2011-41-24-SID81155135229 |