dc.contributor.author |
Safin D. |
|
dc.contributor.author |
Bolte M. |
|
dc.contributor.author |
Shakirova E. |
|
dc.contributor.author |
Babashkina M. |
|
dc.date.accessioned |
2018-09-18T20:07:51Z |
|
dc.date.available |
2018-09-18T20:07:51Z |
|
dc.date.issued |
2009 |
|
dc.identifier.issn |
0277-5387 |
|
dc.identifier.uri |
https://dspace.kpfu.ru/xmlui/handle/net/136806 |
|
dc.description.abstract |
Two N-thiophosphorylated thiosemicarbazides of the common formula RC(S)NHP(S)(OiPr)2 [R = PhNHNH- (1); EtN(NH2)- (2)] have been synthesized and characterized by IR, 1H and 31P spectroscopy, and the single crystal X-ray diffraction method. Single crystal X-ray diffraction studies showed the thiosemicarbazides form both intra- and intermolecular hydrogen bonds, which in turn lead to polymeric chain formation. Moreover, according to the X-ray data of the phenylsubstituted thiosemicarbazide, the formation of intermolecular H⋯η6-phenyl interactions were established. © 2008 Elsevier Ltd. All rights reserved. |
|
dc.relation.ispartofseries |
Polyhedron |
|
dc.subject |
Crystal structures |
|
dc.subject |
Ethylhydrazine |
|
dc.subject |
Phenylhydrazine |
|
dc.subject |
Thiosemicarbazide |
|
dc.title |
The influence of the substituent [PhNHNH- and EtN(NH2)-] on the N-thiophosphorylated thiosemicarbazides RC(S)NHP(S)(OiPr)2 crystal design |
|
dc.type |
Article |
|
dc.relation.ispartofseries-issue |
3 |
|
dc.relation.ispartofseries-volume |
28 |
|
dc.collection |
Публикации сотрудников КФУ |
|
dc.relation.startpage |
501 |
|
dc.source.id |
SCOPUS02775387-2009-28-3-SID59349100824 |
|