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Chiral crystallization of cis-2,3-dichloro-buth-2-ene-1,4-diol

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dc.contributor.author Lodochnikova O.
dc.contributor.author Latypova L.
dc.contributor.author Khakimov R.
dc.contributor.author Kurbangalieva A.
dc.contributor.author Krivolapov D.
dc.contributor.author Litvinov I.
dc.date.accessioned 2018-09-18T20:05:41Z
dc.date.available 2018-09-18T20:05:41Z
dc.date.issued 2013
dc.identifier.issn 0022-4766
dc.identifier.uri https://dspace.kpfu.ru/xmlui/handle/net/136439
dc.description.abstract The X-ray diffraction study of cis-2,3-dichlorobuth-2-ene-1,4-diol (3) obtained by the reduction of 3,4-dichloro-5-ethoxy- and 5-isopropoxi-2(5H)- furanones with lithium aluminum hydride is performed. The crystals of compound 3 are trigonal: a = b = 15.746(9) Å, c = 6.848(4) Å; V = 1470.5(15) Å3, space group P31, Z = 9 (three independent molecules). Independent molecules have identical planar conformation, and hydroxyl groups are located on different sides of the multiple bond plane. The supramolecular motif of the crystal is spirals about the threefold screw axes; the neighboring spirals are linked by OH.O hydrogen bonds. © 2013 Pleiades Publishing, Ltd.
dc.relation.ispartofseries Journal of Structural Chemistry
dc.subject chiral crystallization
dc.subject cis-2,3-dichlorobuth-2-ene-1,4-diol
dc.subject hydrogen bonds
dc.subject supramolecular structure
dc.subject X-ray diffraction study
dc.title Chiral crystallization of cis-2,3-dichloro-buth-2-ene-1,4-diol
dc.type Article
dc.relation.ispartofseries-issue 1
dc.relation.ispartofseries-volume 54
dc.collection Публикации сотрудников КФУ
dc.relation.startpage 213
dc.source.id SCOPUS00224766-2013-54-1-SID84875667620


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  • Публикации сотрудников КФУ Scopus [24551]
    Коллекция содержит публикации сотрудников Казанского федерального (до 2010 года Казанского государственного) университета, проиндексированные в БД Scopus, начиная с 1970г.

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