dc.contributor.author |
Hoentsch J. |
|
dc.contributor.author |
Rosentzweig Y. |
|
dc.contributor.author |
Heinhold D. |
|
dc.contributor.author |
Köhler K. |
|
dc.contributor.author |
Gutjahr M. |
|
dc.contributor.author |
Pöppl A. |
|
dc.contributor.author |
Völkel G. |
|
dc.contributor.author |
Böttcher R. |
|
dc.date.accessioned |
2018-09-17T20:55:00Z |
|
dc.date.available |
2018-09-17T20:55:00Z |
|
dc.date.issued |
2003 |
|
dc.identifier.issn |
0937-9347 |
|
dc.identifier.uri |
https://dspace.kpfu.ru/xmlui/handle/net/134253 |
|
dc.description.abstract |
We describe the design of a pulsed electron nuclear double resonance (ENDOR) spectrometer operating at Q-band frequencies (35 GHz) for studies of transition metal ion complexes in the temperature range between 4.2 and 297 K. Specific features of the spectrometer are a microwave IMPATT generator, a homebuilt cavity, and a commercial Bruker magnet. Standard Davies and Mims ENDOR sequences have been implemented. The performance of the spectrometer is demonstrated for a broad radio frequency range by 1H, 14N, 31P, 133Cs, and 207Pb pulsed ENDOR experiments of Cu 2+, Cr 5+, and V 4+ transition metal ion complexes in both single crystals and disordered materials. |
|
dc.relation.ispartofseries |
Applied Magnetic Resonance |
|
dc.title |
A Q-Band Pulsed ENDOR Spectrometer for the Study of Transition Metal Ion Complexes in Solids |
|
dc.type |
Article |
|
dc.relation.ispartofseries-issue |
2 |
|
dc.relation.ispartofseries-volume |
25 |
|
dc.collection |
Публикации сотрудников КФУ |
|
dc.relation.startpage |
249 |
|
dc.source.id |
SCOPUS09379347-2003-25-2-SID0347063779 |
|