Synthesis of p-tert-butylthiacalix[4]arene with spatially separated phosphoryl and amino groups

dc.contributor.author	Shibaeva K.
dc.contributor.author	Nazarova A.
dc.contributor.author	Kuznetsova D.
dc.contributor.author	Stoikov I.
dc.date.accessioned	2018-04-05T07:09:40Z
dc.date.available	2018-04-05T07:09:40Z
dc.date.issued	2017
dc.identifier.issn	1070-3632
dc.identifier.uri	http://dspace.kpfu.ru/xmlui/handle/net/129886
dc.description.abstract	© 2017, Pleiades Publishing, Ltd. The reactions of p-tert-butylthiacalix[4]arenes containing phthalimide fragments with diethyl-[(p-toluenesulfonyl)oxymethyl)] phosphonate were used to synthesize new phosphonate derivatives in the 1,3-alternate configuration. Hydrolysis and hydrazinolysis of the products gave the corresponding amido- and aminophosphonate thiacalixarene derivatives. 1 H– 1 H NOESY NMR spectroscopy established a 1,3-alternate configuration of the synthesized macrocycles with spatially separated phosphoryl and amino groups.
dc.relation.ispartofseries	Russian Journal of General Chemistry
dc.subject	macrocycles
dc.subject	phosphonates
dc.subject	phosphorylation
dc.subject	thiacalix[4]arene
dc.title	Synthesis of p-tert-butylthiacalix[4]arene with spatially separated phosphoryl and amino groups
dc.type	Letter
dc.relation.ispartofseries-issue	9
dc.relation.ispartofseries-volume	87
dc.collection	Публикации сотрудников КФУ
dc.relation.startpage	2115
dc.source.id	SCOPUS10703632-2017-87-9-SID85031941020

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