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Browsing by Author "Babashkina M."

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Nanoparticles and thin films of silver from complexes of derivatives of N-(diisopropylthiophosphoryl) thioureas

Safin D.; Mdluli P.; Revaprasadu N.; Ahmad K.; Afzaal M.; Helliwell M.; O'Brien P.; Shakirova E.; Babashkina M.; Klein A. (2009)

The derivatives of JV-(diisopropylthiophosphoryl)thiourea RC(S)NHP(S)(OiPr)2 (R = C5H11N, C5H6N2 or C10H7NH 2) followed by their complexation with silver are reported. All complexes are decomposed in hot hexadecylamine ...
New bifunctional N-thiophosphorylated thiourea and 2,5-dithiobiurea derivatives. Crystal structures of R[C(S)NHP(S)(OiPr)2]2 (R = -N(Ph)CH2CH2N(Ph)- and -NHNH-)

Sokolov F.; Safin D.; Bolte M.; Shakirova E.; Babashkina M. (2008)

A new bifunctional N-thiophosphorylated thiourea and 2,5-dithiobiurea of the common formula R[C(S)NHP(S)(OiPr)2]2 [R = -N(Ph)CH2CH2N(Ph)- (H2La); -NHNH- (H2Lb)] have been synthesized and characterized by IR, 1H, 31P ...
Nickel(II) complexes with N-(thio)phosphorylthioureas AdNHC(S)NHP(X)(OiPr)2: Versatile coordination of phosphoryl (X = O) and thiophosphoryl (X = S) derivatives

Safin D.; Sokolov F.; Szyrwiel Ł.; Babashkina M.; Gimadiev T.; Hahn F.; Kozlowski H.; Krivolapov D.; Litvinov I. (2008)

The reaction of the potassium salts of N-(thio)phosphorylated thioureas of the common formula AdN(H)C(S)N(H)P(X)(OiPr)2 (X = O, HLI; X = S, HLII) with the Ni(II) cation in aqueous EtOH leads to [Ni(LI,II)2] chelate complexes. ...
Nitrocellulose membrane, modified by RC(S)NHP(X)(OiPr)2 (X = S, R = PhNH; X = O, R = PhNH, Ph), for sorption extraction of cobalt cations

Sokolov F.; Babashkina M.; Safin D.; Klein A. (2010)

The complexation and extraction properties of RC(S)NHP(X)(OiPr)2 [X = S, R = PhNH (HLI); X = O, R = PhNH (HLII), Ph (HLIII)] towards cobalt cations were studied. The nitrocellulose membrane was used as a carrier for HLI-III. ...
Novel bicyclic hexanuclear copper(I) aggregate: Structure and solid state 31P CPMAS NMR spectra of [(Cu3L3)2] and [Cu(PPh3)2L] complexes of N-(diisopropoxythiophosphinyl)-N′-phenylthiourea (HL)

Sokolov F.; Babashkina M.; Fayon F.; Rakhmatullin A.; Safin D.; Pape T.; Ekkehardt Hahn F. (2009)

A new complex of N-thiophosphorylthiourea PhNHC(S)NHP(S)(OiPr)2 (HL) of formula [(Cu3L3)2] has been synthesized and characterized by single crystal X-ray diffraction, FT-IR, 1H, 31P NMR in solution and by 31P CPMAS NMR ...
Pd[tBuNH(S)NHP(O)(OiPr)2-S]2Cl2 complex as air- and moisture-stable catalyst for palladium catalyzed suzuki cross-coupling reaction

Safin D.; Babashkina M. (2009)

A highly efficient Suzuki cross-coupling reaction between phenyl bromide and phenylboronic acid catalyzed by the palladium complex Pd[tBuNH(S)NHP(O) (OiPr)2-S]2Cl2 in acetonitrile, toluene, THF or DMF has been investigated. ...
Rich magnetic chemistry of cobalt(II) complexes with N-phosphorylthioureas. Crystal structure and solution1H NMR spectral properties

Safin D.; Mlynarz P.; Sokolov F.; Kubiak M.; Ekkehardt Hahn F.; Babashkina M.; Zabirov N.; Galezowska J.; Kozlowski H. (2007)

Structure and magnetic properties of CoII complexes with N-phosphorylthiourea derivatives [RC(S)NHP(O)(OiPr)2] (HL) [Co {Et2NC(S)NP(O)(OzPr)2}2] (1), [Co [(PrNHC(S)NP(O)-(OiPr)2}2] (2), [Co {[/BuNHC(S)NP(O)(OiPr) 2}2] (3), ...
Structure and intramolecular mobility of N-(thio)phosphoryl(thio)amides: XV. Study of structure and intramolecular dynamics of N 3-phenyl-N 1-(diisopropoxythiophosphoryl)thiosemicarbazide in CD 2Cl2 solution by 1H, 13C and 31P NMR spectroscopy

Karataeva F.; Kopytova N.; Sokolov F.; Babashkina M.; Zabirov N. (2009)

Structure and intramolecular transformations of N3-phenyl-N 1-(diisopropoxythiophosphoryl)-thiosemicarbazide in CD 2Cl2 were studied by one- and two-dimensional 1H, 13C and 31P NMR spectroscopy. The combined analysis of ...
Studies on zinc(II) complexes with N-thioacylamidophosphates: X-ray crystal structure of the [Zn(RC(S)NP(O)(OiPr)2)2] (R = NH2, tBuNH, c-C6H11NH)

Safin D.; Sokolov F.; Nöth H.; Babashkina M.; Gimadiev T.; Galezowska J.; Kozlowski H. (2008)

The photoluminescent properties of 17 zinc(II) chelates [Zn(RC(S)NP(O)(OiPr)2-O,S)2] (R = Ph (1a), PhNH (1b), p-BrPh (1c), p-MeOC6H4NH (1d), p-BrC6H4NH (1e), NH2 (1f), iPrNH (1g), tBuNH (1h), Et2N (1i), c-C5H10N (1j), ...
Suzuki cross-coupling reaction catalyzed by the palladium complex Pd[N-MorphC(S)NP(O)(OiPr)2-O,S]2

Safin D.; Babashkina M.; Klein A. (2009)

Suzuki cross-coupling reaction between phenyl bromide and phenylboronic acid, catalyzed by the palladium complex Pd[N-MorphC(S)NP(O)(OiPr) 2-1,5-O,S)]2 in acetonitrile, toluene, THF or DMF has been investigated. Bases ...
Synthesis and characterization of [Me2NC(S)NP(S)(OiPr)2]- complexes of Co(II), Ni(II), Zn(II) and Cd(II)

Safin D.; Bolte M.; Babashkina M.; Kozlowski H. (2010)

Reaction of the potassium salt of N-thiophosphorylthiourea Me2NC(S)NHP(S)(OiPr)2 (HL) with Co(II), Ni(II), Zn(II) and Cd(II) cations in aqueous EtOH leads to M(L-S,S′)2 (ML2) chelate complexes. The structures of the resulting ...
The influence of an intramolecular hydrogen bond on the 1,3-N,S-coordination of crown ether-containing N-phosphorylthiourea with Ni II

Safin D.; Babashkina M.; Klein A.; Sokolov F.; Baranov S.; Pape T.; Hahn F.; Krivolapov D. (2009)

Reaction of the lithium salt of N-phosphorylated thiourea [4′-benzo-15-crown-5]NHC(S)NHP(O)(OiPr)2 (HLI) with NiII leads to the chelate complex [NiLI 2]. The metal center is found in a square-planar N2S2 environment formed ...
The influence of the intramolecular hydrogen bond on the 1,3-N,S- and 1,5-O,S-coordination of N-phosphoryl-N′-(R)-thioureas with Ni(II) and Pd(II)

Sokolov F.; Baranov S.; Safin D.; Hahn F.; Kubiak M.; Pape T.; Babashkina M.; Zabirov N.; Galezowska J.; Kozlowski H.; Cherkasov R. (2007)

Reaction of the potassium salts of N-phosphorylated thioureas of common formula R1-N(H)-C(S)-N(H)-P(O)(OiPr)2 (HA) with Ni II and PdII cations leads to [MA2] chelate complexes (M = NiII, R1 = p-MeOC6H4, p-BrC6H4, t-Bu, ...
The influence of the substituent [PhNHNH- and EtN(NH2)-] on the N-thiophosphorylated thiosemicarbazides RC(S)NHP(S)(OiPr)2 crystal design

Safin D.; Bolte M.; Shakirova E.; Babashkina M. (2009)

Two N-thiophosphorylated thiosemicarbazides of the common formula RC(S)NHP(S)(OiPr)2 [R = PhNHNH- (1); EtN(NH2)- (2)] have been synthesized and characterized by IR, 1H and 31P spectroscopy, and the single crystal X-ray ...
Zn(II), Co(II) and Ni(II) complexes of a phosphorylthiourea derivative of 4-[(EtO)2P(O)CH2]-C6H4-NHC(S)NHP(O) (OiPr)2

Babashkina M.; Safin D. (2010)

The reaction of O,O'-diisopropyl phosphorisothiocyanatidate, (iPrO) 2P(O)NCS, with diethyl-(4-aminobenzyl)phosphonate leads to the new N-phosphorylated thiourea derivative, 4-[(EtO)2P(O)CH 2]-C6H4NHC(S)NHP(O)(OiPr)2 (HL). ...

Now showing items 21-35 of 35

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